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Application of a Graphene Oxide–Carbon Paste Electrode for the Determination of Lead in Rainbow Trout from Central Europe

dc.contributor.authorSMARZEWSKA, SYLWIA
dc.contributor.authorCiesielski, Witold
dc.date.accessioned2015-04-02T12:02:16Z
dc.date.available2015-04-02T12:02:16Z
dc.date.issued2014-06-22
dc.identifier.issn1936-976X
dc.identifier.urihttp://hdl.handle.net/11089/7668
dc.description.abstractIn the presented study, the content of lead in rainbow trout (Oncorhynchus mykiss) samples was examined. Rainbow trout were purchased in Prague (Czech Republic), Lodz (Poland) and Bratislava (Slovakia) from local fish shops and supermarkets belonging to popular chain stores. First, method for quantitative lead determination was developed with very good results (R 2 at 0.9997 in the range of 1.0 × 10−7–7.0 × 10−5 mol L−1 with limit of detection (LOD) and limit of quantification (LOQ) 2.18 × 10−8 and 7.24 × 10−8 mol L−1, respectively). Then, after mineralization, fish samples were analyzed using square wave anodic stripping voltammetry (SWASV) with a graphene oxide–carbon paste electrode (GO–CPE). Lead signals recorded on GO–CPE electrode were 15 % higher than those obtained on bare CPE. The coefficient of variation (CV) was found to be below 5 %. The selectivity of the proposed method was evaluated by the addition of selected heavy metals (zinc, copper, mercury, cobalt, nickel, iron) as possible interferents. Results were confirmed with reference method.pl_PL
dc.description.sponsorshipFinancial support of the grant 506/1123 from the Ministry of Science and Higher Education is gratefully acknowledged.pl_PL
dc.language.isoenpl_PL
dc.publisherSpringerpl_PL
dc.relation.ispartofseriesFood Analytical Methods;2015 8
dc.rightsUznanie autorstwa 3.0 Polska*
dc.rights.urihttp://creativecommons.org/licenses/by/3.0/pl/*
dc.titleApplication of a Graphene Oxide–Carbon Paste Electrode for the Determination of Lead in Rainbow Trout from Central Europepl_PL
dc.typeArticlepl_PL
dc.page.number635–642pl_PL
dc.contributor.authorAffiliationDepartment of Inorganic and Analytical Chemistry, Faculty of Chemistry, University of Lodzpl_PL
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dc.contributor.authorEmailsylwiasmarzewska@gmail.compl_PL


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