8-Phenyl-3,4,6,7,8,8a-hexa­hydro-1H-pyrrolo­[2,1-c][1,4]oxazin-6-one

Małecka, Magdalena; Pasternak, Beata; Leśniak, Stanisław

dc.contributor.author	Małecka, Magdalena
dc.contributor.author	Pasternak, Beata
dc.contributor.author	Leśniak, Stanisław
dc.date.accessioned	2022-01-31T10:11:34Z
dc.date.available	2022-01-31T10:11:34Z
dc.date.issued	2011
dc.identifier.issn	1600-5368
dc.identifier.uri	http://hdl.handle.net/11089/40540
dc.description	In the title compound, C13H15NO2, the hexahydropyrrolo[2,1-c][1,4]oxazine fragment is disordered over two conformations (A and B) in a 0.656 (5):0.344 (5) ratio. The five-membered ring is similarly disordered and adopts an envelope conformation in A, while in B this ring is nearly planar [maximum deviation = 0.088 (1) Å]. The six-membered rings in both A and B exhibit chair conformations. In the crystal, weak intermolecular C—H⋯O hydrogen bonds link the molecules into ribbons propagating in [010].	pl_PL
dc.description.sponsorship	Financial support from University of Łódź (grant No. 505/721/R to MM) is gratefully acknowledged. The authors thank Dr Klaus Harms from Philipps University in Marburg (Germany) for collecting the data.	pl_PL
dc.language.iso	en	pl_PL
dc.publisher	International Union of Crystallography	pl_PL
dc.relation.ispartofseries	Acta Crystallographica Section E: Crystallographic Communications;67
dc.rights	Uznanie autorstwa 4.0 Międzynarodowe	*
dc.rights.uri	http://creativecommons.org/licenses/by/4.0/	*
dc.subject	single-crystal X-ray study	pl_PL
dc.subject	T = 100 K	pl_PL
dc.subject	mean (C–C) = 0.003 A˚	pl_PL
dc.subject	disorder in main residue	pl_PL
dc.subject	R factor = 0.047	pl_PL
dc.subject	wR factor = 0.109	pl_PL
dc.subject	data-to-parameter ratio = 11.7	pl_PL
dc.title	8-Phenyl-3,4,6,7,8,8a-hexahydro-1H-pyrrolo[2,1-c][1,4]oxazin-6-one	pl_PL
dc.type	Article	pl_PL
dc.page.number	o2390	pl_PL
dc.contributor.authorAffiliation	Department of Structural Chemistry and Crystallography, University of Łódź, Tamka 12, PL-91403 Łódź, Poland	pl_PL
dc.contributor.authorAffiliation	Department of Organic and Applied Chemistry, University of Łódź, Tamka 12, PL-91403 Łódź, Poland	pl_PL
dc.contributor.authorAffiliation	Department of Organic and Applied Chemistry, University of Łódź, Tamka 12, PL-91403 Łódź, Poland	pl_PL
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dc.contributor.authorEmail	malecka@uni.lodz.pl	pl_PL
dc.identifier.doi	10.1107/S1600536811032806
dc.relation.volume	9	pl_PL
dc.discipline	nauki chemiczne	pl_PL