8-Phenyl-3,4,6,7,8,8a-hexahydro-1H-pyrrolo[2,1-c][1,4]oxazin-6-one
| dc.contributor.author | Małecka, Magdalena | |
| dc.contributor.author | Pasternak, Beata | |
| dc.contributor.author | Leśniak, Stanisław | |
| dc.date.accessioned | 2022-01-31T10:11:34Z | |
| dc.date.available | 2022-01-31T10:11:34Z | |
| dc.date.issued | 2011 | |
| dc.identifier.issn | 1600-5368 | |
| dc.identifier.uri | http://hdl.handle.net/11089/40540 | |
| dc.description | In the title compound, C13H15NO2, the hexahydropyrrolo[2,1-c][1,4]oxazine fragment is disordered over two conformations (A and B) in a 0.656 (5):0.344 (5) ratio. The five-membered ring is similarly disordered and adopts an envelope conformation in A, while in B this ring is nearly planar [maximum deviation = 0.088 (1) Å]. The six-membered rings in both A and B exhibit chair conformations. In the crystal, weak intermolecular C—H⋯O hydrogen bonds link the molecules into ribbons propagating in [010]. | pl_PL |
| dc.description.sponsorship | Financial support from University of Łódź (grant No. 505/721/R to MM) is gratefully acknowledged. The authors thank Dr Klaus Harms from Philipps University in Marburg (Germany) for collecting the data. | pl_PL |
| dc.language.iso | en | pl_PL |
| dc.publisher | International Union of Crystallography | pl_PL |
| dc.relation.ispartofseries | Acta Crystallographica Section E: Crystallographic Communications;67 | |
| dc.rights | Uznanie autorstwa 4.0 Międzynarodowe | * |
| dc.rights.uri | http://creativecommons.org/licenses/by/4.0/ | * |
| dc.subject | single-crystal X-ray study | pl_PL |
| dc.subject | T = 100 K | pl_PL |
| dc.subject | mean (C–C) = 0.003 A˚ | pl_PL |
| dc.subject | disorder in main residue | pl_PL |
| dc.subject | R factor = 0.047 | pl_PL |
| dc.subject | wR factor = 0.109 | pl_PL |
| dc.subject | data-to-parameter ratio = 11.7 | pl_PL |
| dc.title | 8-Phenyl-3,4,6,7,8,8a-hexahydro-1H-pyrrolo[2,1-c][1,4]oxazin-6-one | pl_PL |
| dc.type | Article | pl_PL |
| dc.page.number | o2390 | pl_PL |
| dc.contributor.authorAffiliation | Department of Structural Chemistry and Crystallography, University of Łódź, Tamka 12, PL-91403 Łódź, Poland | pl_PL |
| dc.contributor.authorAffiliation | Department of Organic and Applied Chemistry, University of Łódź, Tamka 12, PL-91403 Łódź, Poland | pl_PL |
| dc.contributor.authorAffiliation | Department of Organic and Applied Chemistry, University of Łódź, Tamka 12, PL-91403 Łódź, Poland | pl_PL |
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| dc.contributor.authorEmail | malecka@uni.lodz.pl | pl_PL |
| dc.identifier.doi | 10.1107/S1600536811032806 | |
| dc.relation.volume | 9 | pl_PL |
| dc.discipline | nauki chemiczne | pl_PL |
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