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The mechanism of electropolymerization of nickel(ii) salen type complexes

dc.contributor.authorTomczyk, Danuta
dc.contributor.authorUrbaniak, Paweł
dc.contributor.authorSeliger, Piotr
dc.contributor.authorSkrzypek, Slawomira
dc.contributor.authorAndrijewski, Grzegorz
dc.contributor.authorBukowski, Wiktor
dc.contributor.authorBester, Karol
dc.date.accessioned2021-09-10T09:31:09Z
dc.date.available2021-09-10T09:31:09Z
dc.date.issued2017
dc.identifier.issn1369-9261
dc.identifier.urihttp://hdl.handle.net/11089/39022
dc.description.abstractNi(II) complexes with (±)-trans-N,N′-bis(salicylidene)-1,2-cyclohexanediamine ([Ni(salcn)]), and its methyl ([Ni(salcn(Me))]) and tert-butyl ([Ni(salcn(Bu))]) derivatives have been synthesized. Anodic electropolymerization has been used to form electrodes modified by polymer films. FTIR and FTIR ATR methods showed that the obtained films consist of polymers of phenyl–phenyl type. The structure of poly[Ni(salcn)] is built with 1,2,4- and 1,2,3,5-substituted chains. A three-step process of the oxidation of the complexes and their films has been ascertained on the basis of cyclic voltammetry measurements. Furthermore we have also detected the oxidized species which probably serve as intermediates for polymer formation. The influence of the substituent in the phenolate moiety on the type of reaction after which the dimerization and polymerization reaction occurs has been evidenced. Furthermore the substituent dependence on the stability of the phenoxyl radical complex and the Ni(II)-phenoxonium cation has been noticed. For the [Ni(salcn(Bu))] complex, an additional electropolymerization step – the adsorption of the reagent on the electrode surface – has been observed.pl_PL
dc.language.isoenpl_PL
dc.publisherThe Royal Society of Chemistry and the Centre National de la Recherche Scientifiquepl_PL
dc.relation.ispartofseriesNew Journal of Chemistry;41
dc.rightsUznanie autorstwa 4.0 Międzynarodowe*
dc.rights.urihttp://creativecommons.org/licenses/by/4.0/*
dc.subjectelectropolymerizationpl_PL
dc.subjectnickel(ii)pl_PL
dc.subjectNi(II) complexespl_PL
dc.titleThe mechanism of electropolymerization of nickel(ii) salen type complexespl_PL
dc.typeArticlepl_PL
dc.page.number2112-2123pl_PL
dc.contributor.authorAffiliationDepartment of Inorganic and Analytical Chemistry, University of Łódź, 91-403 Łódź, ul.Tamka 12, Polandpl_PL
dc.contributor.authorAffiliationDepartment of Inorganic and Analytical Chemistry, University of Łódź, 91-403 Łódź, ul.Tamka 12, Polandpl_PL
dc.contributor.authorAffiliationDepartment of Inorganic and Analytical Chemistry, University of Łódź, 91-403 Łódź, ul.Tamka 12, Polandpl_PL
dc.contributor.authorAffiliationDepartment of Inorganic and Analytical Chemistry, University of Łódź, 91-403 Łódź, ul.Tamka 12, Polandpl_PL
dc.contributor.authorAffiliationDepartment of Inorganic and Analytical Chemistry, University of Łódź, 91-403 Łódź, ul.Tamka 12, Polandpl_PL
dc.contributor.authorAffiliationFaculty of Chemistry, Rzeszów University of Technology, 35-959 Rzeszów, Al. Powstańców W-wy 6, Polandpl_PL
dc.contributor.authorAffiliationFaculty of Chemistry, Rzeszów University of Technology, 35-959 Rzeszów, Al. Powstańców W-wy 6, Polandpl_PL
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dc.contributor.authorEmailtomczyk@chemia.uni.lodz.plpl_PL
dc.identifier.doi10.1039/c6nj03635j
dc.disciplinenauki chemicznepl_PL


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