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dc.contributor.authorZakrzewski, Robert
dc.contributor.authorZgagacz, W.
dc.contributor.authorUrbaniak, Katarzyna
dc.contributor.authorChwatko, Grażyna
dc.contributor.authorNowicki, A.
dc.description.abstractHydrogen sulfide is a toxic gas involved in the regulation of some essential biological processes. A novel, precise, accurate and rapid method based on high-performance liquid chromatography with diode array detection for the determination of sulfide ions in human urine sample is proposed. The method involves the derivatization of sulfide with pyrylium salts – (2,4,6-triphenylpyrylium hydrogensulfate(VI) (L1) and 4-[p-(N,N-dimethylamino)phenyl]-2,6-diphenylpyrylium chlorate(VII) (LN1). The separation occurs on InfinityLab Poroshell 120 EC C18 column using acetonitrile and phosphate buffer as a mobile phase. The detectors utilized a wavelength of 371 or 580 nm. The calibration curves were linear in the range of 2–150 μmol L−1 and 1–50 μmol L−1 for L1 and LN1 derivatives, respectively. The samples were found to be stable from sample collection to final analysis. The method was successfully applied to samples from apparently healthy volunteers.pl_PL
dc.relation.ispartofseriesJournal of Chromatography B;1157
dc.rightsUznanie autorstwa 4.0 Międzynarodowe*
dc.subjectjon siarczkowypl_PL
dc.subjectsole piryliowepl_PL
dc.subjectwysokosprawna chromatografia cieczowa (HPLC)pl_PL
dc.subjectdetektor diodowy (DAD)pl_PL
dc.subjectSulfide ionspl_PL
dc.subjectPyrylium saltspl_PL
dc.subjectHigh performance liquid chromatography with diode detector (DAD)pl_PL
dc.subjectHuman urine samplepl_PL
dc.titleThe use of high-performance liquid chromatography with diode array detector for the determination of sulfide ions in human urine samples using pyrylium saltspl_PL
dc.contributor.authorAffiliationDepartment of Environmental Chemistry, Faculty of Chemistry, University of Lodz, Polandpl_PL
dc.contributor.authorAffiliationDepartment of Organic and Applied Chemistry, Faculty of Chemistry, University of Lodz, Polandpl_PL
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dc.disciplinenauki chemicznepl_PL

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Uznanie autorstwa 4.0 Międzynarodowe
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